Analytical Instrumentation

  • New ASTM Biodiesel Blend Measuring Method D7861 Validates Use of Portable Analysers

New ASTM Biodiesel Blend Measuring Method D7861 Validates Use of Portable Analysers

Apr 02 2015 Read 2866 Times

The recently-published ASTM method D7861 for measuring biodiesel blend ratios enables users to take full advantage of the speed, convenience and durability provided by portable infrared analysers from Wilks (USA) - a Spectro Scientific Company.

Traditional ASTM D7371 and EN 14078 methods for measuring biodiesel blends require the use of Fourier Transform Infrared (FTIR) spectrometers, equipment that is expensive and requires a level of technical knowledge to operate accurately. The new ASTM method D7861 certifies the use of portable filter-based infrared analysers, such as the Wilks InfraSpec VFA-IR Spectrometer, that are rugged, compact and much better suited for use by on-site personnel in the environment where fuels are blended. The analysers provide a fast, easy-to-use and inexpensive infrared method alternative for measuring biodiesel FAME (Fatty Acid Methyl Esters) blend percentages.

The InfraSpec VFA-IR Spectrometer is a spectral range analyser that employs a linear variable filter and a detector array covering the wavelength range of 5.4-10.8 μm (1850-925 cm-1), making it compliant with the instrument requirements of ASTM D7861. The spectrometer covers a spectral range that enables it to not only measure biodiesel in diesel, but also ethanol in gasoline and water in ethanol. The compact, portable instrument has a simplified PC interface that allows non-technical personnel to make measurements on-site at the blending terminal, as well as at manufacturing facilities or laboratories where an ASTM method is required. The analyser can measure the blend ratio in less than a minute and reads out directly in percent of biodiesel. Measurement range is 0 to 100 percent, with an accuracy of +/- 0.20 percent.

Wilks also offers the rugged, compact, fixed-filter InfraCal 2 ATR-B Biodiesel Blend Analyser. Due to its single wavelength analysis, it is does not comply with D7861; results, however, are comparable with D7371, EN 14078 and the new D7861 method. The InfraCal 2 ATR-B analyser is currently used worldwide by fuel blenders, distributors and regulators. 

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